In conclusion, the work by Ma et al. not only introduces two new and highly promising nano-ELP zeolites but also showcases the potential of MicroED in accelerating the discovery and characterization of complex nano materials. The exceptional structural and catalytic properties of NJU120-1 and NJU120-2 highlight their potential for industrial applications and set a new benchmark for future research in zeolite synthesis and catalysis. This study underscores the importance of interdisciplinary approaches in materials science and provides a roadmap for the advance of next-generation zeolites with enhanced performing and functionality.